Abstract:

This includes the raw Matrix-Assisted Laser Desportion/Ionization (MALDI) Mass Spectrometry (MS) peak integration values used to determine the average molecular weight of the Poly(ethylene glycol) (PEG) star polymers.

Suggested Citation:

Grayson, Scott. 2016. Dataset for: Efficient Synthesis of High Purity Homo-arm and Mikto-arm Poly(ethylene glycol) Stars Using Epoxide and Azide Alkyne Coupling Chemistry. Distributed by: GRIIDC, Harte Research Institute, Texas A&M University–Corpus Christi. doi:10.7266/N77942P0

Publications:

Zhang, B., Zhang, H., Elupula, R., Alb, A. M., & Grayson, S. M. (2013). Efficient Synthesis of High Purity Homo-arm and Mikto-arm Poly(ethylene glycol) Stars Using Epoxide and Azide-Alkyne Coupling Chemistry. Macromolecular Rapid Communications, 35(2), 146–151. doi:10.1002/marc.201300623

Purpose:

Developing CuAAC click protocol for making structurally pure star polymers for enable detailed studies of their physical properties and interactions

Data Parameters and Units:

m/z = mass to charge ratio; Intens = intensity; SN = signal to noise ratio; Quality Fac; Res = resolution; Area = peak area; Rel. intensity = relative intensity; FWHM = full width at half maximum (the resolution of the peak at 50% of the peak height); Chi^2 = chi square; Bk. Peak

Individual Files: